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Anti-Sag Testing of Different Solvent-Based 4420 Versions in Acrylic Emulsion

2025-12-02
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Anjeka Experimental Report

(No:2025103101)

Anjeka4420


Project: Dispersant Comparison

Category: Dispersant Testing

Personnel: R&D Department

Date Submitted: May 28, 2025


1. Objective

Comparison of Anti-Sag Performance in Acrylic Emulsion: Version 4420 with Different Solvent Versions.

 

2. Experimental plan

2.1 Directly incorporate varying proportions of 4420 into the emulsion, mix thoroughly, and test for sagging.

2.2 First prepare a 50% pre-slurry of 4420, then add it to the emulsion and test for sagging.

 

Required Materials:

1. Acrylic emulsion: Double bond DB3422

2. Anjeka 4420 in three solvent versions (NMP/NBP/DMSO)

3. Solvent: BCS

4. Deionized water

 

Required instruments:

1. Flow hanging instrument

 

3.Result and Discussion

 

3.1Procedure

1. After adding different versions of 4420 to the emulsion according to the formulation in Table 1 below, manually mix thoroughly and test the sag thickness.

2. Prepare different versions of the 4420 pre-gel paste according to the formulation in Table 2. Then, following the formulation in Table 3, add the pre-gel paste to the emulsion. Disperse the mixture at 800 rpm for 5 minutes using a high-speed disperser. Finally, measure the sag resistance of the resulting material.

 

3.2 Performance Testing

 

3.2.1 Experimental Formulation

 

Table 1. Formulation for 4420 Additive

4420 content 0.5% 1% 2%
emulsion 100 100 100
4420 0.5 1 2

 

Table 2.4420 Pre-gel Paste Formulation

  4420 BCS Deionized water
Amount 5 3 2

 

Table 3.4420 Pre-gel Paste Addition Formulation

4420 content 0.5% 1% 2%
emulsion 100 100 100
Pre-gel Paste 1 2 4

 

3.2.2 Result and Discussion

 

Comparison of Sag Resistance (μm):

aktueller Firmenfall über Anti-Sag Testing of Different Solvent-Based 4420 Versions in Acrylic Emulsion  0  aktueller Firmenfall über Anti-Sag Testing of Different Solvent-Based 4420 Versions in Acrylic Emulsion  1

aktueller Firmenfall über Anti-Sag Testing of Different Solvent-Based 4420 Versions in Acrylic Emulsion  2

aktueller Firmenfall über Anti-Sag Testing of Different Solvent-Based 4420 Versions in Acrylic Emulsion  3

4. Conclusions

 

1.All three Anjeka 4420 variants demonstrate significant anti-sag performance in this system. When added directly, the NBP-based version shows the best effect. When added as a pre-gel paste, the DMSO-based and NMP-based versions perform similarly, both outperforming the NBP-based version.

 

2.For both the DMSO-based and NMP-based versions, adding them as a pre-gel paste provides a significantly better anti-sag effect compared to direct addition.

 

 

aktueller Firmenfall über Anti-Sag Testing of Different Solvent-Based 4420 Versions in Acrylic Emulsion  0aktueller Firmenfall über Anti-Sag Testing of Different Solvent-Based 4420 Versions in Acrylic Emulsion  0


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